TEACHING LABORATORY
VIRTUAL CHEMLAB
PERFORMANCE LABORATORY
 

 

Redox Analysis Laboratory

Observations

Test
Observations

1) Add a few drops of acidified potassium manganate(VII) solution to solution A.

2) Add a few drops of acidified potassium dichromate(VI) solution to solution A.

3a) Add a few drops of iron(III) chloride solution acidified with dilute hydrochloric acid to solution A.
Stir gently for a few minutes and observe.

3b) Add a few drops of sodium hydroxide solution to the mixture in (a).


Digital image for 3a

View video 3b

4) Add a few drops of iodine solution to solution A.

5a)Add a portion of B add an equal volume of copper(II) sulphate and leave to stand for a few minutes.

b) Add aqueous sodium thiosulphate to the mixture from (a), until no further change.

6) Add acidified hydrogen peroxide solution to 2 cm3 of solution B.

7) Add a spatula of C to 1 cm3 of concentrated hydrochloric acid in a test tube. Warm gently.
Test the gas evolved with damp blue litmus paper.

8) Add 2cm3 of D into iron(II) sulphate solution acidified with dilute sulphuric acid.
Shake for a few minutes and observe, then add a few drops of ammonia solution to the mixture.
9) Add 2 cm3 of D to potassium iodide solution acidified with dilute sulphuric acid.

Conclusion

Unknown A is a/am __________ agent.

Unknown B is a/am __________ agent.

Unknown C is a/am __________ agent.

Unknown D is a/am __________ agent.

 

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